Author: Escudero, C.
Paper Title Page
WEPE15 High Frequency UHV Mechanical X-Ray Beam Chopper 339
 
  • N González, C. Colldelram, C. Escudero, S. Ferrer
    ALBA-CELLS Synchrotron, Cerdanyola del Vallès, Spain
 
  A mechanical chopper* has been designed and built to perform X-ray Absorption Spectroscopy (XAS) experiments with operating liquid electrochemical cells at NAPP end station of ALBA Synchrotron (BL24, CIRCE). When operating the cell, to separate the weak currents induced by the X-ray absorption process at the electrode in contact with the electrolyte (TEY signal) from the faradaic current set between the electrodes, the incoming beam must be chopped at a certain frequency (w). Then, using a lock in amplifier, the signal at this frequency w can be extracted and measured. When the chopper is located in the beam path, it produces pulses with a frequency w, modulating the TEY signal. The chopper developed at ALBA, with variable frequency, improves previous designs which used piezo-actuated choppers constrained to work at fixed oscillating frequencies**. The design consists of a slotted disk that spins around an axis by means of an UHV stepper motor. A LED and photodiode based UHV sensor ensures that frequency drifts do not affect the measurements. The motor is hold by an internally water cooled OFHC support, which allows long duration experiments at high speeds without stopping.
* Patent Registered
** Velasco-Velez et al, Science 2014, 346, 831-834
 
poster icon Poster WEPE15 [4.043 MB]  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-MEDSI2016-WEPE15  
About • paper received ※ 09 September 2016       paper accepted ※ 16 September 2016       issue date ※ 22 June 2017  
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