JLab, Newport News, Virginia, USA
Jefferson Lab, Newport News, Virginia, USA
AASC, San Leandro, California, USA
JLAB, Newport News, Virginia, USA
This study is an on-going research on depositing a Nb film on the internal wall of bulk Nb single cell SRF cavities, via an coaxial energetic condensation (CED) facility at AASC company. The motivation is to firstly create a homoepitaxy-like Nb/Nb film in a scale of a ~1.5GHz RF single cell cavity. Next, through SRF measurement and materials analysis, it might reveal the baseline properties of the CED-type homoepitaxy Nb films. Such knowledge of Nb-Nb homo-epitaxy is useful to create future realistic SRF cavity film coatings, such as hetero-epitaxy Nb/Cu Films, or template-layer-mitigated Nb films. One large-grain, and three fine grain bulk Nb cavity were coated. They went through cryogenic RF measurement. Preliminary results show that the Q0 of a Nb film at 2 K and low rf field, produced by CED, could be close to that of the pre-coated bulk Nb surface (being CBP'ed plus a light EP); but the quality drops rapidly for increasing rf field. We are investigating if the severe Q0-slope is caused by hydrogen incorporation before deposition, or is determined by some structural defects during Nb film growth.
HZB, Berlin, Germany
JLAB, Newport News, Virginia, USA
NCBJ, Świerk/Otwock, Poland
BNL, Upton, Long Island, New York, USA
DESY, Hamburg, Germany
BINP SB RAS, Novosibirsk, Russia
MBI, Berlin, Germany
FZJ, Jülich, Germany
*T. Kamps et al., Proceedings of the 2nd International Particle Accelerator Conference, San Sebastián, Spain, 2011.
JLAB, Newport News, Virginia, USA
Most of the current R&D in SRF is focused on ways to reduce the construction and operating cost of SRF-based accelerators as well as on the development of new or improved cavity processing techniques. The increase in quality factors is the result of the reduction of the surface resistance of the materials. A recent test [*] on a 1.5 GHz single cell cavity made from ingot niobium of medium purity and heat treated at 1400 C in a ultra-high vacuum induction furnace resulted in a residual resistance of ~ 1nanoohm and a quality factor increasing with field up to ~ 5×1010 at a peak magnetic field of 90 mT. In this contribution, we present some results on the investigation of the origin of the extended Q0-increase, obtained by multiple HF rinses, oxypolishing and heat treatment of “all Nb” cavities.
[*] P. Dhakal et al., Phys. Rev. ST Accel. Beams 16, 042001 (2013).
Illinois Institute of Technology, Chicago, IL, USA
JLAB, Newport News, Virginia, USA
Fermilab, Batavia, USA
ANL, Argonne, USA
IIT, Chicago, Illinois, USA
JLAB, Newport News, Virginia, USA
The Hebrew University of Jerusalem, The Racah Institute of Physics, Jerusalem, Israel
In an attempt to correlate the SRF performance of niobium cavities with the superconducting properties, we present the results of the magnetization and ac susceptibility of the niobium used in the superconducting radiofrequency cavity fabrications which were subjected to buffer chemical polishing surface and high temperature heat treatments, typically applied to the SRF cavities fabrications. The analysis of the results show the different surface and bulk ac conductivity for the samples subjected to BCP and HT. Furthermore, the RF surface impedance is measured on the sample using the TE011 microwave cavity for a comparison to the low frequency measurements.
TUP034
NU, Evanston, Illinois, USA
JLAB, Newport News, Virginia, USA
Fermilab, Batavia, USA
UIC, Chicago, USA
NUCAPT, Evanston,, USA
Niobium is the metal of choice for SRF cavities for a linear particle accelerator because it has the highest critical temperature of any element in the periodic table and can be deformed plastically into complex geometries. Differences in the sub-surface chemistry from bulk niobium are believed to determine the high-field Q-drop. In this study, the subsurface chemistry of niobium was characterized utilizing ultraviolet laser-assisted local-electrode atom-probe (LEAP) tomography employing picosecond laser pulsing. The superior spatial resolution and analytical sensitivity of a LEAP tomograph permits us to determine the subsurface composition on an atom-by-atom and atomic {hkl} plane-by-plane basis. The 3-D reconstructions from the LEAP tomographic analyses demonstrate different behaviors for Nb-oxides and Nb-hydrides in pure niobium as well as interactions with structural imperfections, dislocations and grain boundaries in SRF-grade Nb coupon material. Additionally, the chemistry and crystallographic structure of subsurface interstitial atoms were analyzed based on energy shifts of electron energy-loss spectroscopy in conjunction with a scanning transmission electron microscopy.
JLAB, Newport News, Virginia, USA
Centrifugal barrel polishing (CBP) for SRF application is becoming more wide spread as the technique for cavity surface preparation. CBP is now being used in some form at SRF laboratories around the world. Before the process can become as mature as wet chemistry like eletro-polishing (EP) and buffered chemical polishing (BCP) there are many questions which remain unanswered. One of these topics includes the uniformity of removal as a function of cavity shape and material type. In this presentation we show CBP removal rates for various media types on 1.3 GHz TESLA and 1.5 GHz CEBAF large grain niobium cavities, 1.3 GHz TESLA fine grain niobium cavity, and 1.3GHz low surface field copper cavity. The data will also include calculated RF frequency shift modeling non-uniform removal as a function of cavity position and comparing them with CBP results.
WEIOC03
ANL, Argonne, USA
JLAB, Newport News, Virginia, USA
Fermilab, Batavia, USA
IIT, Chicago, Illinois, USA
I will present a summary of the work done over the last 2 years that encompasses both coupons study of thin superconducting films and multilayers and preliminary superconducting RF cavity tests coated by ALD. I will also present results of Nb onto Copper.