MEDSI2018 - List of Authors (Trunk, J.T.)

Paper	Title	Page
THPH19	Engineering Design of the XPD & PDF Beamline Sample Environment for Safe Experimental Use of Hazardous Gases	379
	E. Haas, M. Abeykoon, S. Buda, E.D. Dooryhee, S. Ghose, C. Stelmach, J.T. Trunk BNL, Upton, Long Island, New York, USA
	Funding: U.S. Department of Energy The X-ray Powder Diffraction (XPD) and Pair Distribution Function (PDF) beamlines located at the 28-ID beam port at NSLS-II require a means for safely supplying, containing, and exhausting hazardous gases to and from experimental samples. These beamlines plan to use a wide range of flammable, toxic, and reactive gases for in-situ studies of catalytic and chemical reactions. Since many of the gases are hazardous, a low-cost, robust means is needed to safely supply gases to samples, position the samples quickly, accurately, and remotely, collect scattered X-rays over a wide-angle without distortion, and exhaust the gases safely. Ideally, the sample environment should also allow rapid sample set-up and change-out. The PDF/XPD system includes a sample holder, internal beam stop, sample chamber, and stages that provide eight degrees of freedom. A specially-designed window is also included for maximum X-ray transmission at minimum cost. Sensors, flow metering devices, and circuitry are included to provide proper purging, control hazardous and dilution gas flows, and integrate all of the safeguards needed to assure safe operation. Note to MEDSI reviewers: "Contributed Oral" presentation is indicated above, however a poster presentation can be generated by contacting the author via email at haas@bnl.gov if this is preferred.
DOI •	reference for this paper ※ https://doi.org/10.18429/JACoW-MEDSI2018-THPH19
Export •	reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

Paper

Title

Page

Engineering Design of the XPD & PDF Beamline Sample Environment for Safe Experimental Use of Hazardous Gases

379

E. Haas, M. Abeykoon, S. Buda, E.D. Dooryhee, S. Ghose, C. Stelmach, J.T. Trunk
BNL, Upton, Long Island, New York, USA

Funding: U.S. Department of Energy
The X-ray Powder Diffraction (XPD) and Pair Distribution Function (PDF) beamlines located at the 28-ID beam port at NSLS-II require a means for safely supplying, containing, and exhausting hazardous gases to and from experimental samples. These beamlines plan to use a wide range of flammable, toxic, and reactive gases for in-situ studies of catalytic and chemical reactions. Since many of the gases are hazardous, a low-cost, robust means is needed to safely supply gases to samples, position the samples quickly, accurately, and remotely, collect scattered X-rays over a wide-angle without distortion, and exhaust the gases safely. Ideally, the sample environment should also allow rapid sample set-up and change-out. The PDF/XPD system includes a sample holder, internal beam stop, sample chamber, and stages that provide eight degrees of freedom. A specially-designed window is also included for maximum X-ray transmission at minimum cost. Sensors, flow metering devices, and circuitry are included to provide proper purging, control hazardous and dilution gas flows, and integrate all of the safeguards needed to assure safe operation.
Note to MEDSI reviewers:
"Contributed Oral" presentation is indicated above, however a poster presentation can be generated by contacting the author via email at haas@bnl.gov if this is preferred.

DOI •

reference for this paper ※ https://doi.org/10.18429/JACoW-MEDSI2018-THPH19

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)