Author: Appathurai, N.
Paper Title Page
WEPH01 Evaluation of Anisotropic Simulations & Redesign of the BXDS High Energy Monochromator Bent Laue Diffraction Crystal Holders 199
 
  • M.J.P. Adam, N. Appathurai
    CLS, Saskatoon, Saskatchewan, Canada
 
  The Brockhouse X-ray Diffraction and Scattering Sector (BXDS) High-Energy (HE) beamline includes a bent Laue diffraction monochromator. The BXDS HE monochromator achieves energy ranges of 35keV to 90 keV through the bent Laue diffraction of two silicon crystal wafers. Each wafer (460um & 1000um thick) is bent to achieve specific sagittal radius (Rs); subsequent anticlastic meridional radius (Rm) results from the anisotropic nature of silicon, creating the desired x-ray focusing parameters. During the initial conditioning of the BXDS HE monochromator spurious diffraction patterns were observed indicating that the crystal holder, and crystal integrity failed. Alternative holder designs were evaluated using Finite Element Analysis (FEA; ANSYS) simulations to ensure that appropriate Rs and Rm values were achieved, verification of the crystal holder Rs was completed using contact 3D measurement (FaroArm), and the crystal surface was assessed using 3D optical profiling (Zygo). A superior holder was chosen based on the results, and replaced. The performance of the BXDS HE monochromator has been characterized, indicating the new holder design has achieved x-ray focusing parameters.  
DOI • reference for this paper ※ https://doi.org/10.18429/JACoW-MEDSI2018-WEPH01  
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