LINAC2018 - List of Authors (Nojima, T.)

Paper	Title	Page
TUPO073	Niobium Sample Analysis for Nitrogen Infusion and Doping	506
	T. Konomi, E. Kako, S. Michizono, H. Sakai, K. Umemori KEK, Ibaraki, Japan T. Nagata ULVAC, Inc., Tsukuba, Japan T. Nojima Tohoku University, Sendai, Japan
	KEK has been investigating the better conditions of the heat treatment in nitrogen, which are called as nitrogen doping and nitrogen infusion. We have tried to understand the high gradient performance of the cavity from the analyses of samples which were prepared in the same conditions for the cavity. The main tools are D-SIMS for the depth profile of the elemental concentration, XPS for composition analysis and SQUID magnetometry for the critical DC magnetic field measurement. The difference in the depth profiles of the nitrogen, carbon and oxygen between the heat treatment conditions was observed in vacuum and furnace temperature of nitrogen infusion by D-SIMS and XPS. Such a difference correlates with the vortex penetration field measured by SQUID. In particular, that of nitrogen doping sample was greatly degraded, while that of nitrogen infusion sample was slightly improved. The tendency is similar to the RF high gradient test results. Details of the sample analysis are shown in this presentation.
DOI •	reference for this paper ※ https://doi.org/10.18429/JACoW-LINAC2018-TUPO073
About •	paper received ※ 18 September 2018 paper accepted ※ 21 September 2018 issue date ※ 18 January 2019
Export •	reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)

Paper

Title

Page

Niobium Sample Analysis for Nitrogen Infusion and Doping

506

T. Konomi, E. Kako, S. Michizono, H. Sakai, K. Umemori
KEK, Ibaraki, Japan
T. Nagata
ULVAC, Inc., Tsukuba, Japan
T. Nojima
Tohoku University, Sendai, Japan

KEK has been investigating the better conditions of the heat treatment in nitrogen, which are called as nitrogen doping and nitrogen infusion. We have tried to understand the high gradient performance of the cavity from the analyses of samples which were prepared in the same conditions for the cavity. The main tools are D-SIMS for the depth profile of the elemental concentration, XPS for composition analysis and SQUID magnetometry for the critical DC magnetic field measurement. The difference in the depth profiles of the nitrogen, carbon and oxygen between the heat treatment conditions was observed in vacuum and furnace temperature of nitrogen infusion by D-SIMS and XPS. Such a difference correlates with the vortex penetration field measured by SQUID. In particular, that of nitrogen doping sample was greatly degraded, while that of nitrogen infusion sample was slightly improved. The tendency is similar to the RF high gradient test results. Details of the sample analysis are shown in this presentation.

DOI •

reference for this paper ※ https://doi.org/10.18429/JACoW-LINAC2018-TUPO073

About •

paper received ※ 18 September 2018 paper accepted ※ 21 September 2018 issue date ※ 18 January 2019

Export •

reference for this paper using ※ BibTeX, ※ LaTeX, ※ Text/Word, ※ RIS, ※ EndNote (xml)