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RIS citation export for THPTS026: Effect of Nitric Hydrofluoric Acid Treatment on Brazing of Alumina Ceramics and Pure Titanium

AU  - Kinsho, M.
AU  - Abe, K.
AU  - Kamiya, J.
AU  - Nakamura, T.
ED  - Boland, Mark
ED  - Tanaka, Hitoshi
ED  - Button, David
ED  - Dowd, Rohan
ED  - Schaa, Volker RW
ED  - Tan, Eugene
TI  - Effect of Nitric Hydrofluoric Acid Treatment on Brazing of Alumina Ceramics and Pure Titanium
J2  - Proc. of IPAC2019, Melbourne, Australia, 19-24 May 2019
CY  - Melbourne, Australia
T2  - International Particle Accelerator Conference
T3  - 10
LA  - english
AB  - Alumina ceramics vacuum chamber which is used for the 3GeV rapid-cycling synchrotron (RCS) in J-PARC is composed of alumina duct, titanium (Ti) flanges and Ti sleeves. Before brazing the alumina duct and the Ti sleeves, the Ti sleeves were treated with nitric hydrofluoric acid. The purpose of this study is to clear the effect of this treatment for titanium material. It was cleared by SEM observation that the roughness of the titanium material after the nitric hydrofluoric acid treatment becomes big. It was also measured that the thickness of oxide film on surface of the titanium material was 12.7 nm before treatment and 6.0 nm after treatment. As a result of measuring the wettability of the brazing material which was silver brazing filler metal (Ag: 72%, Cu: 28%) on the Ti surface and the diffusion of the Ti material into the brazing material, it became clear that both the clearing of oxide layer on the alumina ceramics and the vacuum condition of the vacuum heating furnace were important for brazing between alumina ceramics and pure titanium.
PB  - JACoW Publishing
CP  - Geneva, Switzerland
SP  - 4161
EP  - 4163
KW  - vacuum
KW  - electron
KW  - controls
KW  - experiment
KW  - gun
DA  - 2019/06
PY  - 2019
SN  - 978-3-95450-208-0
DO  - DOI: 10.18429/JACoW-IPAC2019-THPTS026
UR  - http://jacow.org/ipac2019/papers/thpts026.pdf
ER  -