SRF2013 - List of Authors (Kang, D.)

Paper	Title	Page
MOP033	Quality Assurance and Acceptance Testing of Niobium Material for Use in the Construction of the Facility for Rare Isotope Beams (FRIB) at Michigan State University (MSU)	174
	C. Compton, D. Miller FRIB, East Lansing, Michigan, USA T.R. Bieler, D. Kang Michigan State University, East Lansing, Michigan, USA S.K. Chandrasekaran, N.T. Wright MSU, East Lansing, USA
	Funding: Work supported by US DOE Cooperative Agreement DE-SC0000661 and Michigan State University Niobium is the current material of choice for the fabrication of superconducting radio frequency (SRF) cavities used in SRF based accelerators. Although niobium specifications for this application have been well established, material properties of as-received materials can still vary substantially. As required for the FRIB accelerator, large volumes (60,000 lbs) of niobium materials (sheet, tube, and flange) have been contracted to several niobium vendors. The FRIB cavity designs require very large niobium sheets, increasing the difficulty in fabrication and potential for contamination. FRIB has developed and initiated plans to control niobium specifications and perform incoming acceptance checks to ensure quality is maintained. Acceptance results from the first niobium shipment will be presented, looking at several production lots from the same vendor and across multiple vendors. Non-conforming results were observed and will be discussed including follow-up investigations and mitigation strategies to improve quality of future shipments.

TUP016	Effects of Processing History on Damage Layer Evolution in Large Grain Nb Cavities	455
	D. Kang, T.R. Bieler Michigan State University, East Lansing, USA C. Compton FRIB, East Lansing, Michigan, USA
	Funding: This work was supported by the U.S. Department of Energy, Office of High Energy Physics, through Grant No. DE-S0004222. Previous cavity tests identified a strong dependence of achievable accelerating gradients on the amount of material removed from the surface. Samples extracted from the iris and the equator of a half cell fabricated by Jefferson Lab using large grain Nb were examined to identify underlying mechanisms. Electron backscattered diffraction (EBSD) was used to measure the crystal orientations on the cross sections of the samples. Results demonstrated the presence of a surface damage layer, which contained higher dislocation content than the bulk due to the deep drawing process. The depth of the damage layer depends on crystal orientations, and damage to the iris is more severe than at the equator. From the EBSD data, the damage depth was estimated to be about 100 microns. The samples were then heat treated at 800°C and 1000°C, and the same areas were examined again for the effects of heat treatment on the healing of the damage layer. While the damage layer accounts for some of the performance gain from chemical surface removal, the depth of the damage layer in polycrystalline cavities remains an open question.

TUP017	Study of Slip and Dislocations in High Purity Single Crystal Nb for Accelerator Cavities	461
	D. Kang, D.C. Baars, T.R. Bieler Michigan State University, East Lansing, USA C. Compton FRIB, East Lansing, Michigan, USA
	Funding: This work was supported by the U.S. Department of Energy, Office of High Energy Physics, through Grant No. DE-S0004222. SRF Cavities can be formed by deep drawing slices from Nb ingots with large grains. Crystal orientation dependent slip system activities affect the shape change of ingot slices during deep drawing, and form a dislocation substructure that affects subsequent recrystallization and ultimately, cavity performance. Two groups of single crystal tensile specimens with different orientations were extracted from a large grain ingot slice. The first group was deformed monotonically to 40% engineering strain. Analysis revealed that slip was preferred on {112} planes. The second group was heat treated at 800°C for two hours, and then deformed incrementally to 40% engineering strain using an in situ tensile stage. Crystal orientations and surface images were recorded at each increment of deformation. Results indicate that the heat treated group had lower yield strengths, and the details of slip activity differed in the annealed samples. Active slip systems were investigated and compared to the first group. Direct observations of dislocations were performed in selected specimens using electron channeling contrast imaging, to determine how slip affects the dislocation substructure.

Paper

Title

Page

Quality Assurance and Acceptance Testing of Niobium Material for Use in the Construction of the Facility for Rare Isotope Beams (FRIB) at Michigan State University (MSU)

174

C. Compton, D. Miller
FRIB, East Lansing, Michigan, USA
T.R. Bieler, D. Kang
Michigan State University, East Lansing, Michigan, USA
S.K. Chandrasekaran, N.T. Wright
MSU, East Lansing, USA

Funding: Work supported by US DOE Cooperative Agreement DE-SC0000661 and Michigan State University
Niobium is the current material of choice for the fabrication of superconducting radio frequency (SRF) cavities used in SRF based accelerators. Although niobium specifications for this application have been well established, material properties of as-received materials can still vary substantially. As required for the FRIB accelerator, large volumes (60,000 lbs) of niobium materials (sheet, tube, and flange) have been contracted to several niobium vendors. The FRIB cavity designs require very large niobium sheets, increasing the difficulty in fabrication and potential for contamination. FRIB has developed and initiated plans to control niobium specifications and perform incoming acceptance checks to ensure quality is maintained. Acceptance results from the first niobium shipment will be presented, looking at several production lots from the same vendor and across multiple vendors. Non-conforming results were observed and will be discussed including follow-up investigations and mitigation strategies to improve quality of future shipments.

TUP016

Effects of Processing History on Damage Layer Evolution in Large Grain Nb Cavities

455

D. Kang, T.R. Bieler
Michigan State University, East Lansing, USA
C. Compton
FRIB, East Lansing, Michigan, USA

Funding: This work was supported by the U.S. Department of Energy, Office of High Energy Physics, through Grant No. DE-S0004222.
Previous cavity tests identified a strong dependence of achievable accelerating gradients on the amount of material removed from the surface. Samples extracted from the iris and the equator of a half cell fabricated by Jefferson Lab using large grain Nb were examined to identify underlying mechanisms. Electron backscattered diffraction (EBSD) was used to measure the crystal orientations on the cross sections of the samples. Results demonstrated the presence of a surface damage layer, which contained higher dislocation content than the bulk due to the deep drawing process. The depth of the damage layer depends on crystal orientations, and damage to the iris is more severe than at the equator. From the EBSD data, the damage depth was estimated to be about 100 microns. The samples were then heat treated at 800°C and 1000°C, and the same areas were examined again for the effects of heat treatment on the healing of the damage layer. While the damage layer accounts for some of the performance gain from chemical surface removal, the depth of the damage layer in polycrystalline cavities remains an open question.

TUP017

Study of Slip and Dislocations in High Purity Single Crystal Nb for Accelerator Cavities

461

D. Kang, D.C. Baars, T.R. Bieler
Michigan State University, East Lansing, USA
C. Compton
FRIB, East Lansing, Michigan, USA

Funding: This work was supported by the U.S. Department of Energy, Office of High Energy Physics, through Grant No. DE-S0004222.
SRF Cavities can be formed by deep drawing slices from Nb ingots with large grains. Crystal orientation dependent slip system activities affect the shape change of ingot slices during deep drawing, and form a dislocation substructure that affects subsequent recrystallization and ultimately, cavity performance. Two groups of single crystal tensile specimens with different orientations were extracted from a large grain ingot slice. The first group was deformed monotonically to 40% engineering strain. Analysis revealed that slip was preferred on {112} planes. The second group was heat treated at 800°C for two hours, and then deformed incrementally to 40% engineering strain using an in situ tensile stage. Crystal orientations and surface images were recorded at each increment of deformation. Results indicate that the heat treated group had lower yield strengths, and the details of slip activity differed in the annealed samples. Active slip systems were investigated and compared to the first group. Direct observations of dislocations were performed in selected specimens using electron channeling contrast imaging, to determine how slip affects the dislocation substructure.