Author: Inman, M.E.
Paper Title Page
TUIOC02 Bipolar EP: Electropolishing without Fluorine in a Water Based Electrolyte 404
 
  • A.M. Rowe, A. Grassellino
    Fermilab, Batavia, USA
  • T.D. Hall, M.E. Inman, S.T. Snyder, E.J. Taylor
    Faraday Technology, Inc., Clayton, USA
 
  Funding: Operated by Fermi Research Alliance, LLC under contract No. De-AC02-07CH11359 with the United States Department of Energy
For more than thirty years, preparing superconducting RF cavities for high performance has required the use of dangerous and ecologically damaging chemicals. Reducing the personnel and environmental risks associated with using these chemicals is a priority at Fermilab. Therefore, Fermilab pursued a project to adapt a non-hazardous and relatively benign bipolar electropolishing technique to SRF cavities that Faraday Technology, Inc. developed. Faraday initially developed this electropolishing technique to polish metal alloys used in automotive and semiconductor components as well as medical devices and implants. By modifying the cathodic/anodic interaction via a pulse forward/pulse reverse technique, Fermilab and Faraday Technology demonstrate the capability to polish 1.3 GHz single-cell cavities utilizing an aqueous 10% sulfuric acid electrolyte. We present the development of bipolar EP for single-cell 1.3 GHz cavities and show the results from vertical tests achieving gradients greater than 40 MV/m.
 
slides icon Slides TUIOC02 [1.251 MB]  
 
TUP054 Electropolishing of Niobium SRF Cavities in Low Viscosity Aqueous Electrolytes Without Hydrofluoric Acid 540
 
  • E.J. Taylor, T.D. Hall, M.E. Inman, S.T. Snyder
    Faraday Technology, Inc., Clayton, USA
  • A.M. Rowe
    Fermilab, Batavia, USA
 
  Funding: U.S. DOE Purchase order No. 594128
Electropolishing of niobium materials and cavities is conventionally conducted in high viscosity electrolytes consisting of concentrated sulfuric and hydrofluoric acid. The use of these dangerous and ecologically damaging chemicals requires careful attention to safety protocol to avoid harmful worker exposure and environmental damage. In this poster we present an approach based on bipolar voltage fields enabling the use of low viscosity water based electrolytes without hydrofluoric acid for electropolishing of niobium materials. The subtleties of the bipolar electropolishing process vis-a-vis conventional electropolishing will be presented.