SRF2013 - List of Authors (Checchin, M.)

Paper

Title

Page

Purification of 6 GHz Cavities by Induction Heating

419

A.A. Rossi, A. Battistello, M. Checchin, V. Palmieri, S. Stark, F. Stivanello, R.K. Thakur, G. Yu
INFN/LNL, Legnaro (PD), Italy

We have developed an innovative technique for purification of bulk-Nb 6GHz RF cavities under ultra-high vacuum (UHV) system. The main advantages of 6 GHz bulk-Nb cavities are saving cost, materials and time to collect statistics of surface treatments and RF test. Cavities are RF tested before and after high temperature treatment under UHV conditions. Induction heating method is used to anneal the cavity at temperatures higher than 2000°C and close to the melting point of Nb for less than a minute while few seconds at maximum temperature. Before RF test and UHV annealing, the surface treatment processes like tumbling, chemical, electro-chemical (such as BCP and EP), ultrasonic cleaning and high pressure rinsing (HPR) have been employed. This kind of Nb 6 GHz cavity purification allow to reduce hydrogen, oxygen and other elemental impurities content, which effects on cavity Q-factor degradation, by a rapid annealing over 2000°C and a subsequent rapid reduction at room temperature.

Slides TUIOC05 [42.171 MB]

TUP030

Elimination of post annealing chemistry: a route to high Q cavities and processing simplification

A. Grassellino, A.C. Crawford, R.D. Kephart, O.S. Melnychuk, A. Romanenko, A.M. Rowe, D.A. Sergatskov, M. Wong
Fermilab, Batavia, USA
M. Checchin
INFN/LNL, Legnaro (PD), Italy
Y. Trenikhina
IIT, Chicago, USA

Funding: Fermilab is operated by Fermi Research Alliance, LLC under Contract No. DE-AC02-07CH11359 with the United States Department of Energy.
We investigate the effect of high temperature treatments followed by only high-pressure water rinse (HPR) of superconducting radio frequency (SRF) niobium cavities. The objective is to provide a cost effective alternative to the typical cavity processing sequence, by eliminating the material removal step post furnace treatment while preserving or improving the RF performance. The studies have been conducted in the temperature range 800-1000C for different conditions of the starting substrate: large grain and fine grain, electro-polished (EP) and centrifugal barrel polished (CBP) to mirror finish. An interesting effect of the grain size on the performances is found. Cavity results and samples characterization show that furnace contaminants cause poor cavity performance, and a practical solution is found to prevent surface contamination. Extraordinary values of residual resistances ~ 1 nOhm and below are then consistently achieved for the contamination-free cavities. We explore the addition of a small partial pressure of gas during the anneal to further increase the cavity quality factor by reducing the BCS resistance.

Paper	Title	Page
TUIOC05	Purification of 6 GHz Cavities by Induction Heating	419
	A.A. Rossi, A. Battistello, M. Checchin, V. Palmieri, S. Stark, F. Stivanello, R.K. Thakur, G. Yu INFN/LNL, Legnaro (PD), Italy
	We have developed an innovative technique for purification of bulk-Nb 6GHz RF cavities under ultra-high vacuum (UHV) system. The main advantages of 6 GHz bulk-Nb cavities are saving cost, materials and time to collect statistics of surface treatments and RF test. Cavities are RF tested before and after high temperature treatment under UHV conditions. Induction heating method is used to anneal the cavity at temperatures higher than 2000°C and close to the melting point of Nb for less than a minute while few seconds at maximum temperature. Before RF test and UHV annealing, the surface treatment processes like tumbling, chemical, electro-chemical (such as BCP and EP), ultrasonic cleaning and high pressure rinsing (HPR) have been employed. This kind of Nb 6 GHz cavity purification allow to reduce hydrogen, oxygen and other elemental impurities content, which effects on cavity Q-factor degradation, by a rapid annealing over 2000°C and a subsequent rapid reduction at room temperature.
	Slides TUIOC05 [42.171 MB]

TUP030	Elimination of post annealing chemistry: a route to high Q cavities and processing simplification
	A. Grassellino, A.C. Crawford, R.D. Kephart, O.S. Melnychuk, A. Romanenko, A.M. Rowe, D.A. Sergatskov, M. Wong Fermilab, Batavia, USA M. Checchin INFN/LNL, Legnaro (PD), Italy Y. Trenikhina IIT, Chicago, USA
	Funding: Fermilab is operated by Fermi Research Alliance, LLC under Contract No. DE-AC02-07CH11359 with the United States Department of Energy. We investigate the effect of high temperature treatments followed by only high-pressure water rinse (HPR) of superconducting radio frequency (SRF) niobium cavities. The objective is to provide a cost effective alternative to the typical cavity processing sequence, by eliminating the material removal step post furnace treatment while preserving or improving the RF performance. The studies have been conducted in the temperature range 800-1000C for different conditions of the starting substrate: large grain and fine grain, electro-polished (EP) and centrifugal barrel polished (CBP) to mirror finish. An interesting effect of the grain size on the performances is found. Cavity results and samples characterization show that furnace contaminants cause poor cavity performance, and a practical solution is found to prevent surface contamination. Extraordinary values of residual resistances ~ 1 nOhm and below are then consistently achieved for the contamination-free cavities. We explore the addition of a small partial pressure of gas during the anneal to further increase the cavity quality factor by reducing the BCS resistance.