Paper | Title | Page |
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TUPPO086 | Surface Characterization of Niobium Samples Electropolished Together with Real Cavities | 441 |
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We report the results of surface characterization of niobium samples electropolished together with single-cell niobium cavities. These witness samples were located in three regions of the cavity, namely at the equator, the iris and the beam-pipe respectively. Auger electron spectroscopy (AES) was utilized to probe the chemical composition of the topmost four atomic layers. Scanning electron microscopy with energy dispersive x-ray for elemental analysis (SEM/EDX) was used to observe the surface topography and chemical composition at the micrometer scale. A few atomic layers of sulfur (S) were found covering the samples non-uniformly. Niobium oxide granules with a sharp geometry were observed on every sample. Some Nb-O granules appeared to also contain sulfur. |