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| WE5PFP054 | HOM Survey of the First CEBAF Upgrade Style Cavity Pair | 2123 |
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Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177. For the planned CEBAF upgrade ten new cryomodules are required to increase the beam energy to the envisaged 12 GeV. Extensive cavity and cryomodule R&D has been done previously, including the installation of a new cryomodule dubbed “Renascence” in CEBAFs north linac in 2007. It houses both seven-cell low loss and high gradient type of cavities thereby serving as a testbed to address and cope with crucial technological challenges. Based on this experience a final iteration on the upgrade cavity has been performed to improve various aspects of HOM-damping and thermal stability. Two such cavities have been produced and qualified. A thorough cavity HOM-survey has been performed to verify the integrity of the cavities and to guarantee the impedance requirements of each crucial HOM. This paper details the results of HOM-surveys performed for the first two upgrade style low loss cavities tested both individually in a vertical Dewar and horizontally in a dedicated cavity pair cryomodule. The safety margin to the worst beam break-up scenario at 12 GeV has been concluded. |
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| WE5PFP055 | Improved Performance of JLab 7-Cell Cavities by Electropolishing | 2126 |
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Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177 The great majority of experience in niobium SRF cavity processing at Jefferson Lab is with BCP etching. This has been used on CEBAF cavities and others totaling over 500 in number. With improved process quality control, field emission is now largely controlled and other factors limit performance. All of the prototype cavities developed for the 12 GeV upgrade, although meeting minimum requirements, have demonstrated a Q-drop in the 17 23 MV/m range that is not remedied by 120 C bake. Most of these cavities received >250 micron removal by BCP etch. Three of these cavities are being electropolished using the protocol under development within ILC R&D activities. The first such cavity was transformed from Q = 3 ·1010 at 17 MV/m to quench from 1010 at 35 MV/m. The details of this and two subsequent electropolished JLab 7-cell cavities will be reported. |
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| WE5PFP057 | Integrated Surface Topography Characterization of Variously Polished Niobium for Superconducting Particle Accelerators | 2132 |
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Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177. As SRF cavities approach fundamental material limits, there is increased interest in understanding the details of topographical influences on performance limitations. Micro-and nano-roughness are implicated in direct geometrical field enhancements and complications of the composition of the 50 nm surface layer in which the super-currents flow. Interior surface etching (BCP/EP) to remove mechanical damage leaves surface topography, including pits and protrusions of varying sharpness. These may promote RF magnetic field entry, locally quenching superconductivity, so as to degrade cavity performance. A more incisive analysis of surface topography than the widely-used average roughness is needed. In this study, a power spectral density (PSD) approach based on Fourier analysis of surface topography data acquired by both stylus profilometry and atomic force microscopy (AFM) is being used to distinguish the scale-dependent smoothing effects. The topographical evolution of the varied starting state Nb surface (CBP/ EBW) as a function of applied etching, polishing steps and conditions is reported, resulting in a novel qualitative and quantitative description of Nb surface topography. |
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| WE5PFP058 | Basic Electropolishing Process Research and Development in Support of Improved Reliable Performance SRF Cavities for the Future Accelerators | 2135 |
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Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177. Future accelerators require unprecedented cavity performance, which is strongly influenced by interior surface nanosmoothness. Electropolishing is the technique of choice to be developed for high-field superconducting radiofrequency cavities. Electrochemical impedance spectroscopy (EIS) and related techniques point to the electropolishing mechanism of Nb in a sulfuric and hydrofluoric acid electrolyte of controlled by a compact surface salt film under F- diffusion-limited mass transport control. These and other findings are currently guiding a systematic characterization to form the basis for cavity process optimization, such as flowrate, electrolyte composition and temperature. This integrated analysis is expected to provide optimum EP parameter sets for a controlled, reproducible and uniform surface leveling for Nb SRF cavities. |
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| WE5PFP060 | Buffered Electropolishing – A New Way for Achieving Extremely Smooth Surface Finish on Nb SRF Cavities to be Used in Particle Accelerators | 2141 |
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Funding: Notice: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177. A new surface treatment technique for niobium (Nb) Superconducting Radio Frequency (SRF) cavities called Buffered Electropolishing (BEP) has been developed at JLab. It was found that BEP could produce the smoothest surface finish on Nb samples ever reported in the literature. Experimental results revealed that the Nb removal rate of BEP could reach as high as 4.67 μm/min. This is significantly faster* than that of the conventional electropolishing technique employing an acid mixture of HF and H2SO4. An investigation is underway to determine the optimum values for all relevant BEP parameters so that the high quality of surface finish achieved on samples can be realized within the geometry of an elliptical RF cavity. Toward this end, single cell Nb cavities are being electropolished by BEP at both CEA-Saclay and JLAB. These cavities will be RF tested and the results will be reported through this presentation. *Xiangyang Lu et al, to be published. |
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| WE5PFP061 | Commissioning of the SRF Surface Impedance Characterization System at Jefferson Lab | 2144 |
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Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177. Much remains to be learned regarding the details of SRF performance effects with material variation, including niobium treated in different ways, and different bulk/thin film materials that are fabricated under different conditions. A facility that can measure small samples’ RF properties in a range of 0~180mT magnetic field and 2~20k temperature is necessary in order to answer this question. The Jefferson Lab surface impedance characterization (SIC) system has been designed to attempt to meet this requirement. The SIC system uses a sapphire-loaded cylindrical Nb cavity at 7.5GHz with 50mm diameter flat sample placed on a non-contacting end plate and a calorimetric technique to directly measure the rf dissipation in the sample in response to known rf fields over ~1 cm2. We report on the commissioning of this system and its first uses for characterizing materials. Preliminary tests with Nb thin film sample sputtered on Cu substrate, and bulk Nb sample have been done at low field. The presently available hardware is expected to enable tests up to 20 mT peak magnetic field on the sample CW. Paths to higher field tests have been identified. |
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| WE5PFP062 | Surface Topography of "Hotspot" Regions from a Single Cell SRF Cavity | 2147 |
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Funding: Authored by Jefferson Science Associates, LLC under U.S. DOE Contract No. DE-AC05-06OR23177. SRF cavities are observed to be limited by non-linear localized effects. The variation of local material parameters between "hot" and "cold" spots is thus of intense interest. Such locations were identified in a BCP etched large-grain single-cell cavity and removed for examination by high resolution electron microscopy (SEM), electron-back scattering diffraction microscopy (EBSD), and scanning Auger electron spectroscopy (SAM). Pits with clear crystal facets were observed on both "Hotspot" and "Coldspot" specimens. The pits were found in-grain and on "Y"-shaped junction of three crystals. They are interpreted as etch pits induced by surface crystal defects (e.g., dislocations). All "Coldspots" examined had obvious low density of etching pits or very shallow tri-crystal boundary junction. EBSD revealed crystal structure surrounding the pits via crystal phase orientation mapping. This study suggests a mechanism by which BCP etching creates pits on large-grain Nb cavity surfaces and sharp-edged topography in fine-grain Nb. Field enhancements at very deep, sharp and densely populated etching pits may then cause distributed hotspots and limit cavity performance. |
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| TU5PFP002 | Atomic Layer Deposition for SRF Cavities | 803 |
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Funding: DOE/OHEP We have begun using Atomic Layer Deposition (ALD) to synthesize a variety of surface coatings on coupons and cavities as part of an effort to produce rf structures with significantly better performance and yield than those obtained from bulk niobium, The ALD process offers the possibility of conformally coating complex cavity shapes with precise layered structures with tightly constrained morphology and chemical properties. Our program looks both at the metallurgy and superconducting properties of these coatings, and also their performance in working structures. Initial results include: 1) evidence from point contact tunneling showing magnetic oxides can be a significant limitation to high gradient operation, 2) experimental results showing the production sharp niobium/oxide interfaces from a high temperature bake of ALD coated Al2O3 on niobium surfaces, 3) results from ALD coated structures. |