Author: Sawabe, M.
Paper Title Page
MOPC092 Effect of Current Densities on Sulfur Generation at Electropolished Niobium Surface 292
 
  • P.V. Tyagi
    Sokendai, Ibaraki, Japan
  • H. Hayano, S. Kato, M. Nishiwaki, T. Noguchi, T. Saeki, M. Sawabe
    KEK, Ibaraki, Japan
 
  We conducted a series of electropolishing (EP) experiments in aged EP acid with high (≈50 mA/cm2) and low (≈30 mA/cm2) current densities on Nb surfaces. The experiments were carried out both for laboratory coupons and a real Nb single cell cavity with six witness samples located at three typical positions (equator, iris and beam pipe). All the samples surface were investigated by XPS (x-ray photoelectron spectroscopy), SEM (scanning electron microscope) and EDX (energy dispersive x-ray spectroscopy). The surface analysis showed the EP with a high current density produced a huge amount sulfate particles at Nb surface whereas the EP with a low current density is very helpful to mitigate sulfate at Nb surface in both the experiments.